1. Raw Material Preparation
Petroleum coke/Needle coke: Premium low-sulfur, low-ash coke as aggregate
Coal tar pitch: Medium-temperature or modified pitch as binder (softening point 80-90℃)
Additives: Optional graphite scraps or anti-oxidants
Key Controls:: Ash content ≤0.5%; Volatile matter 8-12%; True density ≥2.10g/cm³
2. Crushing & Screening
Multi-stage crushing process: Primary crushing (50-80mm) via jaw crusher
Secondary crushing (10-20mm) via roller crusher
Fine grinding (0.075-0.5mm/200 mesh) via ball mill
Screening System: Vibrating screens (4-6 particle size grades)
Optimized aggregate/fine powder ratio (3:7~4:6)


3. Kneading & Forming
Process Flow: Dry mixing: Preheat aggregates at 150-180℃ for 2-3 hours
Wet mixing: Add liquid pitch (180-200℃), knead for 40-60 mins
Cooling: Cool to 110-130℃ before forming
Forming Methods: Extrusion (vertical/horizontal ramming)
Vibration forming (for large electrodes)
Molding (special shapes)
4. Baking Process
Temperature Profile: Room temp→300℃ (5-7 days, volatile removal)
300→800℃ (3-5 days, binder coking)
800→1200℃ (2-3 days, pre-graphitization)
Key Parameters: Baking cycle: 25-35 days
Peak temperature: 1100-1250℃
Packing material: Metallurgical coke (anti-oxidation)
5. Impregnation Treatment
(High-density electrodes require 2-3 cycles)
Preheating: 200-300℃ under vacuum (≤10kPa)
Pressure impregnation: 0.5-1.5MPa for 2-4 hours
Re-baking: Follow baking process
Weight Gain: 1st impregnation: 8-12%
2nd impregnation: 5-8%
6. Graphitization
Acheson Furnace Process
Loading capacity: 50-80 tons/furnace
Heating curve: 0-24h: Slow ramp to 800℃
24-72h: Rapid heating to 2600-2800℃
Soaking: 12-24 hours
Cooling cycle: 7-10 days
Quality Controls:
Post-graphitization resistivity ≤6.5μΩ·m
Temperature uniformity ±50℃
7. Machining
Processing Steps: Turning: Diameter tolerance ±1mm
Threading: ISO/NPT standards (pitch 8-12mm)
End finishing: Flatness ≤0.1mm/m
Surface treatment: Optional anti-oxidation coating
Precision Standards:
Straightness ≤1mm/m
Concentricity ≤0.5mm
Thread clearance ≤0.2mm
8. Quality Inspection
Test Items: Physical properties: Density, resistivity, flexural strength
Dimensional inspection: CMM verification
Ultrasonic testing: Internal defect detection
Joint test: Torque resistance ≥3000N·m
Certifications:
Complies with GB/T 3072-2018
ISO 9001 certified
9. Packaging & Storage
Moisture-proof: PE film + desiccants
Transportation: Dedicated steel frames
Storage: Humidity ≤60%, max 3-layer stacking
Process Highlights:
"Low-Temperature Prolonged Baking" minimizes cracks
Multi-grade particle optimization enhances density
Precise graphitization ensures uniform properties
Full-process MES traceability
(HP/UHP grades available per customer requirements)
Products Parameters
|
Item |
Unit |
RP |
HP |
UHP |
||||
|
≤∅400 |
≥∅450 |
≤∅400 |
≥∅450 |
≤∅400 |
≥∅450 |
|||
|
Electric Resistivity |
Electrode |
μΩ*m |
≤8.5 |
≤9.0 |
≤6.0 |
≤6.5 |
≤5.0 |
≤5.5 |
|
Nipple |
≤6.5 |
≤6.5 |
≤5.5 |
≤5.5 |
≤4.5 |
≤4.5 |
||
|
Transverse Strength |
Electrode |
MPa |
≥8.0 |
≥7.0 |
≥10.5 |
≥10.5 |
≥15.0 |
≥15.0 |
|
Nipple |
≥16.0 |
≥16.0 |
≥20.0 |
≥20.0 |
≥22.0 |
≥22.0 |
||
|
Young's Modulus |
Electrode |
Gpa |
≤9.3 |
≤12.0 |
≤14.0 |
|||
|
Nipple |
≤14.0 |
≤16.0 |
≤18.0 |
|||||
|
Bulk Density |
Electrode |
g/cm3 |
≥1.54 |
≥1.65 |
≥1.68 |
|||
|
Nipple |
≥1.69 |
≥1.73 |
≥1.76 |
|||||
|
Coefficient of Termal Expansion (100℃﹣600℃) |
Electrode |
100-6/℃ |
≤2.5 |
≤2.0 |
≤1.5 |
|||
|
Nipple |
≤2.0 |
≤1.6 |
≤1.2 |
|||||
|
Ash |
% |
≤0.3 |
≤0.2 |
≤0.2 |
||||
